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Synthesis and Characterization of Iodo Derivatives of Bis-salphen Complexes

Melia Lacaze 1 Nathalie Saffon‐merceron 2 Fabien Silly 3 Jacques Bonvoisin 4, *
* Corresponding author
1 CEMES-GNS - Groupe NanoSciences
CEMES - Centre d'élaboration de matériaux et d'études structurales
3 LEPO - Laboratoire d'Electronique et nanoPhotonique Organique
SPEC - UMR3680 - Service de physique de l'état condensé, IRAMIS - Institut Rayonnement Matière de Saclay
Abstract : Two new iodo derivatives of bis-salphen zinc complexes [salphen = N,N’-bis(salicylideneimine)-1,2-diaminobenzene] have been synthesized and fully characterized. The 1H NMR, 13C NMR, IR, UV-Vis, TGA, elemental analysis and MALDI mass spectral data of these complexes are presented. In addition, X-Ray single crystal diffraction analysis of complex 1 has been recorded. These two compounds present a great potential interest for generating 2D covalent organic nanoarchitecture.
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Melia Lacaze, Nathalie Saffon‐merceron, Fabien Silly, Jacques Bonvoisin. Synthesis and Characterization of Iodo Derivatives of Bis-salphen Complexes. Journal of Molecular Structure, Elsevier, In press, ⟨10.1016/j.molstruc.2020.129319⟩. ⟨hal-02949087⟩

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